This study focuses on the petrography and palynological analyses of the Upper Cretaceous sedimentary facies in
Ankpa, North Central Nigeria. The primary aim was to unravel the organic composition, age and the prevailed
peleoenvironmental conditions of the sediments. The methodology employed towards achieving these was the
application of palynological analysis on 20 samples composed of coal and claystone, recovered from the coal
mine. The samples were subjected to series of laboratory procedures such as decarbonisation with dilute HCl,
sample digestion with hydrofouric acid, sieving of the samples with 10µ mesh, oxidation, heavy liquid separation,
rinsing with ethanol, and mounting of the macerals on glass slides. Subsequently, the organic residues were
microscopically analyzed using an OPTIKA G-150 microscope, facilitating the identification and counting of
pollen, spores, dinoflagellates, and algae. In establishing the age and paleoenvironment of deposition of the
sediments, marker species and stratigraphically significant forms were considered. The stratigraphic interval 0.05
to 23.8 m is composed of claystone at the upper part with dominant underlying coal beds. The palynostratigraphy
of the coal measure was defined based on recovery of marker palynomorphs which belongs to Spinizonocolpites
baculatus Assemblage Zone, characterized by the co-occurrences of Constructipollenites ineffectus, Auriculiidites
sp., Proxapertites operculatus, Longapertites microfoveolatus, Retidiporites magdalenensis, Syncolporites
marginatus, Cingulatisporites ornatus, Buttinea andreevi, Proteacidites sp., and Inaperturopollenites sp., all
indicative of Late Maastrichtian age. The co-occurrence of terrestrially derived miospores and marine
peridinacean form of dinoflagellates such as Andalusiella polymorpma senegalinium sp., and Oligosphaeridium
sp. are indicative of fluviomarine setting. However, evidence of sea level fluctuation was noticed whereby the
coal interval of about 12.4 m which is rich in pollen, spores, dinoflagellates, and algae suggest a shift in coastline
further landward compared to the overlying claystone. The ETA Zuma coal is characteristically similar to other
coal deposits such as Mamu Coal Measure, dated late Maastrichtian on the basis of similarity in palynomorph
assemblage.